Carbamic acid, cyclopropyl-, 1,1-dimethylethyl ester (9CI)
Carbamic acid, cyclopropyl-, 1,1-dimethylethyl ester (9CI)
CAS: 132844-48-5
Molecular Formula: C8H15NO2
Carbamic acid, cyclopropyl-, 1,1-dimethylethyl ester (9CI) - Names and Identifiers
| Name | Carbamic acid, cyclopropyl-, 1,1-dimethylethyl ester (9CI) |
| Synonyms | N-Boc-cyclopropylamine tert-Butyl cyclopropylcarbamate tert-butyl cyclopropylcarbamatato Cyclopropylamine, N-BOC protected N-Cyclopropylcarbamic acid tert-butyl ester CarbaMic acid, cyclopropyl-, 1,1-diMethylethyl ester Carbamic acid, cyclopropyl-, 1,1-dimethylethyl ester (9CI) |
| CAS | 132844-48-5 |
| InChI | InChI=1/C8H15NO2/c1-8(2,3)11-7(10)9-6-4-5-6/h6H,4-5H2,1-3H3,(H,9,10) |
Carbamic acid, cyclopropyl-, 1,1-dimethylethyl ester (9CI) - Physico-chemical Properties
| Molecular Formula | C8H15NO2 |
| Molar Mass | 157.21 |
| Density | 1.01±0.1 g/cm3(Predicted) |
| Boling Point | 228.6±7.0 °C(Predicted) |
| Flash Point | 92.033°C |
| Vapor Presure | 0.073mmHg at 25°C |
| pKa | 12.74±0.20(Predicted) |
| Storage Condition | 2-8°C |
| Refractive Index | 1.463 |
| MDL | MFCD09701238 |
Carbamic acid, cyclopropyl-, 1,1-dimethylethyl ester (9CI) - Reference Information
| preparation | with chloroethyl ketone as the starting material, then the carbonyl group was reduced by sodium borohydride, Wittig-Horner-Wadsworth cyclopropanation reaction, hydrolysis, after reacting with ethyl chloroformate to form anhydride, it reacts with sodium azide to generate acyl azide compound. Finally, it is rearranged by curtis to generate cyclopropanamide, and then protected by Boc to obtain target compound N-BOC-cyclopropylamine. N-BOC-synthesis of cyclopropylamine reaction formula as shown below: |
Last Update：2024-04-09 02:00:02
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